Property | Value |
Name | Reverse phase High Performance Liquid Chromatographic determination of residual Carbendazim (fungicide) in raw and cooked Indian cereals and pulses |
Description | Research article:- K. Karunambigai*, C. Saravanan, C. A. Sureshkumar, K. Kaveri, M. Thamizhmozhi. Aadhibhagawan College of Pharmacy, Rantham, Cheyyar-604407, Thiruvannamalai, Tamil Nadu, India.
Abstract:- The present work describe a reverse phase HPLC method for line quantification of carbandazim in raw and cooked Indian Cereals as pulses the retention time of carbandazim is 2.85minutes in RP HPLC using 10%V/V phosphate butter in acetonitrile water in ratio 17.37:46 as mobile phase and c18 (5u 250X4.6mm)by hypersil column as stationary phase . The effluent was monitored by UV detection at 230nm the method was validated for accuracy, precision, specificity in this study 15 samples of cereals by pulses of different varieties were analyzed for residues of carbandazim in raw as well as cooked forms. The maximum residual limit for cerbandazim residues in cereals and pulses is 0.5 mg/kg. The analyzed amount of carbandazim residues in raw sample of cereals and pulses was 0.0320-18.8171 mg/kg by collected samples 0.003-0.6776 mg/kg. The carbandazin plots were within range of 0.1 to 100 mg /ml (R.0.9995), the observed percentage recovery of carbandazim was found to be 90.09-102-82% which indicated good accuracy and reproducibility of the method.
Key words:- RP-HPLC, Carbendazim, Cereals, Pulses, Determination. |
Filename | K. Karunambigai et al.pdf |
Filesize | 297.75 kB |
Filetype | pdf (Mime Type: application/pdf) |
Creator | admin |
Created On: | 09/09/2012 00:00 |
Viewers | Everybody |
Maintained by | Editor |
Hits | 8198 Hits |
Last updated on | 10/22/2012 06:44 |
Homepage | |
CRC Checksum | |
MD5 Checksum |